Journal
MOLECULES
Volume 15, Issue 2, Pages 813-823Publisher
MDPI
DOI: 10.3390/molecules15020813
Keywords
solvent-free; sustainable procedure; microwave; Knoevenagel; catalysis
Funding
- Ministry of Education - Morocco [D13/57]
- CNRST-Morocco
- CNRS
- UNS
- Conseil Regional PACA
- MAE
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A sustainable Knoevenagel condensation of a series of aldehydes with malononitrile and ethyl cyanoacetate is described. The process is based on the combination of microwave activation and hydroxyapatite catalysis under solvent-free conditions. Products are obtained in and high yields after short reaction times. The effects of the specific surface of porous calcium hydroxyapatite and microwave activation are discussed.
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