4.1 Article

Synthesis of nanocrystalline birnessite and cryptomelane by microwave hydrothermal treatment

Journal

RUSSIAN JOURNAL OF INORGANIC CHEMISTRY
Volume 60, Issue 11, Pages 1299-1303

Publisher

MAIK NAUKA/INTERPERIODICA/SPRINGER
DOI: 10.1134/S0036023615110108

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Funding

  1. Russian Foundation for Basic Research [14-29-04100]

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Effect of reaction medium acidity on the phase composition and morphology of manganese dioxide obtained by microwave hydrothermal treatment was studied. Conditions for the preparation of single-phase nanocrystalline polymorphs of manganese dioxide, birnessite and cryptomelane, were revealed. The obtained samples were characterized by X-ray diffraction, Raman spectroscopy, and scanning electron microscopy.

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