Journal
MEAT SCIENCE
Volume 84, Issue 3, Pages 484-490Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.meatsci.2009.10.002
Keywords
Phthalates; Ham sausage; Packaging film; Migration; GC-MS; Solid-phase extraction
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Funding
- Science and Technology Department of Zhejiang Province of China [2007F70009, 2007R40G2070022]
- K.C. Wong Magna Fund in Ningbo University
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A gas chromatography-mass spectrometry assay was developed and successfully applied for the determination of phthalates in ham sausage migrated from packaging film. The phthalates studied were dimethyl phthalate (DMP), diethyl phthalate (DEP), dibutyl phthalate (DBP), benzylbutyl phthalate (HP), bis(2-ethylhexyl) phthalate (DEHP) and di-n-octyl phthalate (DNOP), with dibutyl adipate (DBA) as internal standard. The sample pre-treatments included extraction with n-hexane, solvent evaporation and reconstitution with acetonitrile before and after solid-phase extraction (SPE). The extraction and cleaning up procedure was carried Out with cartridges containing dimethyl butylamine groups, which showed extraction efficiencies over 87.3%. The calibration curves obtained were linear with correlation coefficients greater than 0.99. The method proved to be accurate and precise for the six phthalates used. It was successfully applied to a Study on the migration of phthalates from packaging PVC film into ham Sausage. (C) 2009 Elsevier Ltd. All rights reserved.
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