Journal
REVISTA BRASILEIRA DE FARMACOGNOSIA-BRAZILIAN JOURNAL OF PHARMACOGNOSY
Volume 25, Issue 2, Pages 177-179Publisher
SOC BRASILEIRA FARMACOGNOSIA
DOI: 10.1016/j.bjp.2015.03.006
Keywords
Philippine propolis; Tetragonula biroi; Propolin A; Propolin E; Propolin H; Glyasperin A
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Funding
- De La Salle University Science Foundation through the University Research Coordination Office
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Chemical investigation of the dichloromethane extracts of the propolis collected from bee (Tetragonula biroi Friese) hives in San Roque, Sorsogon, Philippines afforded propolin A (1), propolin E (2), propolin H (3), glyasperin A (4), squalene, a mixture of lupeol, alpha-amyrin and beta-amyrin, and another mixture of urs-12-en-3-one, olean 12 en 3 one and lup-12-en-3-one. The structures of 2-4 were elucidated by extensive 1D and 2D (COSY, HSQC, and HMBC) NMR spectroscopy, while 1 was identified by comparison of its NMR data with 2. (C) 2015 Sociedade Brasileira de Farmacognosia. Published by Elsevier Editora Ltda. All rights reserved.
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