4.5 Article

Compact low temperature scanning tunneling microscope with in-situ sample preparation capability

Journal

REVIEW OF SCIENTIFIC INSTRUMENTS
Volume 86, Issue 9, Pages -

Publisher

AMER INST PHYSICS
DOI: 10.1063/1.4931761

Keywords

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Funding

  1. National Science Foundation in the USA [DMR-1506678]
  2. Office of Naval Research in the USA [ONR-N00014-14-1-0330]
  3. Welch Foundation [F1672]
  4. National Research Foundation of Korea [NRF-2013R1A1A1008724, NRF-2009-0093818, NRF-2014R1A4A1071686]
  5. Direct For Mathematical & Physical Scien
  6. Division Of Materials Research [1506678] Funding Source: National Science Foundation
  7. National Research Council of Science & Technology (NST), Republic of Korea [K15018] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)
  8. National Research Foundation of Korea [21A20131100002, 2009-0093818, 2013R1A1A1008724] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)

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We report on the design of a compact low temperature scanning tunneling microscope (STM) having in-situ sample preparation capability. The in-situ sample preparation chamber was designed to be compact allowing quick transfer of samples to the STM stage, which is ideal for preparing temperature sensitive samples such as ultra-thin metal films on semiconductor substrates. Conventional spring suspensions on the STM head often cause mechanical issues. To address this problem, we developed a simple vibration damper consisting of welded metal bellows and rubber pads. In addition, we developed a novel technique to ensure an ultra-high-vacuum (UHV) seal between the copper and stainless steel, which provides excellent reliability for cryostats operating in UHV. The performance of the STM was tested from 2 K to 77 K by using epitaxial thin Pb films on Si. Very high mechanical stability was achieved with clear atomic resolution even when using cryostats operating at 77 K. At 2 K, a clean superconducting gap was observed, and the spectrum was easily fit using the BCS density of states with negligible broadening. (C) 2015 AIP Publishing LLC.

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