4.3 Article

Four-Dimensional Morphological Evolution of an Aluminum Silicon Alloy Using Propagation-Based Phase Contrast X-ray Tomographic Microscopy

Journal

MATERIALS TRANSACTIONS
Volume 55, Issue 1, Pages 161-164

Publisher

JAPAN INST METALS & MATERIALS
DOI: 10.2320/matertrans.M2013225

Keywords

X-ray tomographic microscopy; aluminum-silicon alloy; propagation-based phase contrast; microstructural characterization; coarsening

Funding

  1. DOE
  2. U.S. Department of Energy, Office of Basic Energy Sciences, Division of Materials Sciences and Engineering [DE-FG02-99ER45782]
  3. AFOSR [FA9550-12-1-0458]
  4. 176th Committee on Process Created Materials Function of the Japan Society for the Promotion of Science (JSPS)

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Four-dimensional propagation-based phase contrast X-ray tomographic microscopy experiments were performed on an Aluminum-29.9 mass% Silicon alloy during coarsening. Using propagation-based phase contrast, changes in the three-dimensional morphology of primary silicon particles were captured and the resulting evolution of the microstructure is discussed. While morphologies at earlier times are complex, faceted and highly interconnected, the morphologies at later times are less faceted but remain quite complex.

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