Journal
MATERIALS SCIENCE AND ENGINEERING B-ADVANCED FUNCTIONAL SOLID-STATE MATERIALS
Volume 176, Issue 18, Pages 1435-1447Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.mseb.2011.08.001
Keywords
Thermoplastic polyurethane; Multi-walled carbon nanotube; Nanocomposites; Morphology; Thermomechanical properties; Melt intercalation
Funding
- Extra Mural Research Division II (EMR-II), Human Resource Development Group (HRDG), Council of Scientific and Industrial Research (CSIR), New Delhi, India [22(0410)/06/EMR-II]
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The multi-walled carbon nanotube (MWNT) reinforced thermoplastic polyurethane (TPU) nanocomposites were prepared through melt compounding method followed by compression molding. The spectroscopic study indicated that a strong interfacial interaction was developed between carbon nanotube (CNT) and the Tpu matrix in the nanocomposites. The microscopic observation showed that the CNTs were homogeneously dispersed throughout the TPU matrix well apart from a few clusters. The results from thermal analysis indicated that the glass transition temperature (T-g) and storage modulus (E') of the nanocomposites were increased with increase in CNTs content and their thermal stability were also improved in comparison with pure TPU matrix. The theological analysis showed the low frequency plateau of shear modulus and the shear thinning behavior of the nanocomposites. The electrical behaviors of the nanocomposites are increased with increase in weight percent (wt%) of CNT loading. The mechanical properties of nanocomposites were substantially improved by the incorporation of CNTs into the TPU matrix. (C) 2011 Elsevier B.V. All rights reserved.
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