Journal
MATERIALS SCIENCE AND ENGINEERING B-ADVANCED FUNCTIONAL SOLID-STATE MATERIALS
Volume 171, Issue 1-3, Pages 109-115Publisher
ELSEVIER
DOI: 10.1016/j.mseb.2010.03.082
Keywords
2-aminophenoxazin-3-one; Multi-walled carbon nanotubes; Pd nanoparticles; Methanol oxidation; Fuel cells
Funding
- Natural Science Foundation of Guangxi Province [0728043]
- Guangxi Ministry of Education and Innovation Plan in Graduate Education of Guangxi Province [2009106020703M49]
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A simple and rapid synthesis method to prepare well-dispersed Pd nanoparticles on 2-aminophenoxazin-3-one (APZ) functionalized multi-walled carbon nanotubes (Pd/APZ-MWCNTs) is presented. Scanning electron microscopy (SEM), transmission electron microscopy (TEM). X-ray diffraction (XRD), Fourier transforms infrared spectrometry (FT-IR) as well as Raman spectrum are used for the catalysts characterization. The electrocatalytic properties of the Pd/APZ-MCWNTs catalyst for methanol oxidation have been investigated by cyclic voltammetry and chronoamperometry methods. In contrast to the Pd nanoparticles supported on acid-treated MWCNTs and carbon black catalysts, the electrochemical results demonstrate that Pd/APZ-MCWNTs exhibit better electrocatalytic activities and stability, mainly due to the uniform dispersion and small particle size of Pd nanoparticles on the APZ-MWCNTs supports. The results imply that the Pd/APZ-MWCNTs catalyst shows the better electrocatalytic performances and has a promising application potential in fuel cells. (C) 2010 Elsevier B.V. All rights reserved.
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