Microstructure and mechanical property of in-situ nano-particle strengthened ferritic steel by novel internal oxidation

A novel route of fabricating nano-particles strengthened ferrite steel was investigated in this study. Rather than by externally adding nano-oxide powders, we adopted the endogenous method of controlling oxide reaction and solute concentration distribution in the process of deoxidization to obtain a high density of in-situ nano-oxide particles homogeneously dispersed in the ferrite matrix in melt. The microstructure and tensile properties of these materials had been investigated to clarify the interrelation between the composition, microstructure and mechanical properties. Transmission electron microscopy (TEM) analysis indicated that these nano-particles were titanium oxides, which have a positive effect on optimizing inclusions and refining grains. Tensile tests revealed that these titanium oxide particles play an important role in increasing the yield strength. The steel has yield strength of 711 MPa, approximately three times higher than that of conventional plain carbon structural steels, and its ultimate tensile strength reaches 810 MPa with an elongation-to-failure value of 22%. Precipitation hardening and grain refinement hardening are the dominant factors responsible for yield strength increasing in this steel. (C) 2014 Elsevier B.V. All rights reserved.