Journal
MATERIALS RESEARCH BULLETIN
Volume 50, Issue -, Pages 307-311Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.materresbull.2013.11.031
Keywords
Oxides; Chemical synthesis; Crystal growth; X-ray diffraction
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Funding
- GF Science and Technology Innovation Fund of Chinese Academy of Sciences [CXJJ-11-M44]
- National Natural Science Foundation of China [51002154, 51272253]
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Mesoporous MgO particles have been synthesized through a novel template-free hydrothermal co-precipitation method using a Mg(NO3)(2) solution as the magnesium source and NaCO3 as precipitant. The samples were characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy, and N-2 adsorption-desorption analysis. The results indicate that the MgO samples have a disordered mesoporous structure, a large BET surface area, and a large pore volume. The effect of reaction temperature on the MgO product BET surface area was studied. A possible formation and crystal growth mechanism for mesoporous MgO is proposed. (C) 2013 Elsevier Ltd. All rights reserved.
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