Journal
MATERIALS LETTERS
Volume 111, Issue -, Pages 211-213Publisher
ELSEVIER
DOI: 10.1016/j.matlet.2013.08.077
Keywords
Ti3SiC2; Ceramics; Powder; Molten salt; Microstructure
Funding
- Open Project of State Key Laboratory Cultivation Base for Nonmetal Composites and Functional Materials
- Project of Science and Technology Department of Sichuan Province [2010JY0090]
- Postgraduate Innovation Fund Project by Southwest University of Science and Technology [13ycjj07]
- Project of Laboratory for Extreme Conditions Matter Properties, Southwest University of Science and Technology [11zxjk03]
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Ti3SiC2 powders were successfully obtained by the molten salt method using NaCl as the flux. The influences of synthetic temperatures and flux/powders weight ratio. on the phase and morphology of Ti3SiC2 powders were investigated. The results indicated that the synthetic temperature of Ti3SiC2 was about 150 degrees C lower than that reported by other methods. The Ti3SiC2 powders obtained by the molten salt method at 1200 degrees C were uniform and the particle size was about 1-2 mu m. The content of Ti3SiC2 increased as flux/powders ratio increased to 1:1 while the further increment of the ratio made the content decreases obviously. (C) 2013 Elsevier B.V. All rights reserved.
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