Journal
MATERIALS LETTERS
Volume 65, Issue 3, Pages 579-582Publisher
ELSEVIER SCIENCE BV
DOI: 10.1016/j.matlet.2010.11.001
Keywords
Molybdenum oxides; Vanadium oxide; Rods; Hydrothermal synthesis; Metastable phase; Hexagonal structure; Magnetic properties
Funding
- Deutsche Forschungsgemeinschaft [KL 1824/2]
- BMBF via LIB
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(VO)(0.09)V0.18Mo0.82O3 center dot 0.54H(2)O microrods have been synthesized for the first time via a hydrothermal treatment of aqueous peroxomolybdic acid and vanadyl sulfate. The compound crystallizes in hexagonal rods with space group P6(3), and lattice constants a = 10.586 angstrom, and c = 3.698 angstrom. The single crystalline rods exhibit diameters of 1-2 mu m and lengths up to 45 mu m. A variety of techniques, including X-ray diffraction, scanning electron microscopy, high-resolution transmission electron microscope. Fourier-transform infrared spectroscopy, differential scanning calorimetry and static magnetometry were used to characterize the product. (C) 2010 Elsevier B.V. All rights reserved.
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