Journal
RESEARCH ON CHEMICAL INTERMEDIATES
Volume 42, Issue 3, Pages 2303-2315Publisher
SPRINGER
DOI: 10.1007/s11164-015-2150-y
Keywords
Poly(vinylpyrrolidone) (PVP); Poly(vinylpyrrolidinium) perchlorate {[PVPH]ClO4}; Polyhydroquinoline derivatives; Hantzsch condensation; Solvent-free conditions
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Funding
- University of Guilan Research Councils
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A green approach for the promotion of the synthesis of Hantzsch products using poly(vinylpyrrolidinium) perchlorate {[PVPH]ClO4} as a new modified polymeric catalyst in the absence of solvent is reported. The title catalyst is easily prepared and characterized using a variety of techniques including infrared spectra, X-ray diffraction, thermal gravimetric analysis, scanning electron microscopy, pH analysis, and Hammett acidity function. Some of the advantages of this novel synthetic method are: easy preparation of the catalyst, short reaction times, high to excellent yields of the products, simple and easy work-up procedure, and reusability of the catalyst.
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