Journal
MATERIALS CHEMISTRY AND PHYSICS
Volume 134, Issue 2-3, Pages 921-924Publisher
ELSEVIER SCIENCE SA
DOI: 10.1016/j.matchemphys.2012.03.091
Keywords
Oxides; Chemical synthesis; Ultrasonic techniques; Phase transitions
Categories
Funding
- Program for New Century Excellent Talents in University [NCET-10-0360]
- Fundamental Research Funds for the Central Universities, Hunan university
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Well-crystallized manganese ferrite nanoparticles with mean size of 20 nm were synthesized at low temperature (<= 100 degrees C) by ultrasound wave-assisted solid-liquid reaction ball milling technique without subsequent calcination. MnO2 were used as the raw material and iron milling balls with diameter of 1.0-1.5 mm were used. As a comparison, solid-liquid reaction ball milling without ultrasonic wave assistance and the effects of different milling balls were also investigated. The results showed that, this technique is simple, environmentally friendly and energy-saving for nanocrystal synthesis. (c) 2012 Elsevier B.V. All rights reserved.
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