Journal
MAGNETIC RESONANCE IN CHEMISTRY
Volume 49, Issue 1, Pages 46-49Publisher
WILEY
DOI: 10.1002/mrc.2706
Keywords
NMR; H-1 NMR; C-13 NMR; 2D NMR; steroids; Sinularia brassica; coral
Funding
- National High Technology Development Project (863 Project) [2006AA09Z408]
- Provincial Scientific Fund of Guangdong [06025194, 2005A30503001]
- National Natural Scientific Fund, China [20772048]
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Two new steroids, named 4 alpha, 22-dimethyl-Cholest-22-en-3 beta-ol (1) and 4 alpha-methyl-Cholest-7,22-dien-3 beta-ol (2), along with two known steroids, were isolated from the soft coral Sinularia brassica. The structures of the new compounds were determined on the basis of extensive spectroscopic data (MS, H-1 and C-13 NMR, H-1-H-1 COSY, C-13-H-1 COSY, HMBC and NOESY) analysis. Copyright (C) 2010 John Wiley & Sons, Ltd.
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