Journal
MACROMOLECULAR RAPID COMMUNICATIONS
Volume 30, Issue 1, Pages 34-38Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/marc.200800607
Keywords
click chemistry; Cu(I) catalyst; NMR; polyamine network; supported catalysis; supports; transition metal chemistry
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Funding
- Ghent University
- Research Foundation - Flanders (FWO)
- Belgian Program on Interuniversity Attraction Poles
- STIPOMAT ESF-program
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A novel heterogeneous copper(I) catalyst system, which is based on readily available poly(ethyleneimine), has been used as a recyclable catalyst for Cu(I) catalyzed click 1,3 dipolar cycloaddition reactions of azides and alkynes in organic media. Branched poly(ethyleneimine) was first methylated and then cross-linked with 1,9-dibromononane. Subsequently, after the immobilization of Cu(I)Br, this system was applied for heterogeneous copper catalyzed click chemistry of a few model reagents and polymeric compounds.
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