Journal
MACROMOLECULAR MATERIALS AND ENGINEERING
Volume 298, Issue 12, Pages 1282-1293Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/mame.201300024
Keywords
composites; electrospinning; fibres; medical applications; microgels
Funding
- Volkswagen Stiftung
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In this work microgel-PVA composite fibres are prepared by means of an electrospinning process using aqueous solutions of poly(vinyl alcohol) (PVA) and poly(N-vinylcaprolactam)-based microgels. The optimal parameters are defined to fabricate homogenous composite fibres in which the microgels are embedded into a PVA matrix. It is demonstrated that the fibres can be physically and chemically crosslinked. The fibre morphology is visualised and its properties investigated by differential scanning calorimetry, DSC, thermo-gravimetric analysis, TGA, and isothermal moisture sorption analysis. The results show that the thermo-sensitive properties of the microgels are retained inside the fibres and that the degree of swelling and the moisture sorption kinetics can be tuned by changing the temperature.
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