Journal
MACROMOLECULAR MATERIALS AND ENGINEERING
Volume 297, Issue 10, Pages 985-993Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/mame.201100414
Keywords
cellulose; compatibiliztion; composites; poly(e-caprolactone)
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A comparative study of the preparation and properties of composites of PCL with cellulose microfibres (CFs) containing butanoic-acid-modified cellulose (CB) or PCL grafted with maleic anhydride/glycidyl methacrylate as compatibilizers, is reported. The composites are obtained by melt mixing and analyzed using SEM, DSC, TGA, XRD, FT-IR, NMR and tensile tests. An improved interfacial adhesion is observed in all compatibilized composites, as compared to PCL/CF. The crystallization behavior and crystallinity of PCL is largely affected by CF and CB content. Composites with PCL-g-MAGMA display higher values of tensile modulus, tensile strength and elongation at break.
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