Journal
LETTERS IN ORGANIC CHEMISTRY
Volume 5, Issue 8, Pages 655-658Publisher
BENTHAM SCIENCE PUBL LTD
DOI: 10.2174/157017808786857552
Keywords
Ytterbium perfluorooctanesulfonate; Amberlyst A-21; polymer supported catalyst; 1,5-benzodiazepines; fluorous-solvent-free
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Funding
- Nature and Science Foundation of Jiangsu Province [BK2007592]
- National Defense Committee of Science and Technology of China [40406020301]
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Amberlyst-21, a kind of well-known and cheap polymeric material, was treated with ytterbium perfluorooctanesulfonate [Yb(OPf)(3)] giving a reagent with a ytterbium loading of 1.34 (wt %). The polymer-supported fluorous ytterbium catalyses the highly efficient synthesis of 1,5-benzodiazepine derivatives. The catalyst can be recovered by simple filtration under fluorous-solvent-free conditions and used again without a significant loss of catalytic activity.
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