Journal
LANGMUIR
Volume 29, Issue 25, Pages 8054-8060Publisher
AMER CHEMICAL SOC
DOI: 10.1021/la3046498
Keywords
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Funding
- Bundesministerium fur Bildung und Forschung via the LIB2015 alliance [03SF0340/03SF0397]
- DFG [KL 1824/2, KL1824/5]
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Microwave-assisted hydrothermal synthesis was used to grow LiMnPO4 micro- and nanocrystals from acetate precursors. By appropriate adjustment of the precursor concentration and the pH-value of the reactant, the product composition and purity along with the crystal size can be manipulated, resulting in particle-dimensions from around 10 mu m down to a few 100 nm. Prisms and plates with hexagonal basal faces as well as cuboid and rod-like particles were produced. The effects on the crystal morphology as well as on the materials texture and agglomeration tendency are discussed and a comprehensive agglomeration phase diagram is constructed.
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