Journal
JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
Volume 109, Issue 3, Pages 1473-1479Publisher
SPRINGER
DOI: 10.1007/s10973-012-2212-y
Keywords
Aqueous thermolysis; Trans-zinc glycinate complex; Thermal analysis
Funding
- Indian Space Research Organization (ISRO)
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ZnO and different atomic percentages of Cu-doped ZnO nanocrystallites have been prepared by aqueous thermolysis method using Glycine as a fuel and encapsulating agent. Mechanism and formation of intermediate products have been given for the first time. All the findings given are for samples annealed at 800 A degrees C. XRD of nanocrystalline ZnO and Cu-ZnO has been indexed to hexagonal wurtzite structure. Influence of temperature on thermal properties of gel precursor and Cu-doped ZnO nanoparticles have been investigated using thermogravimetric and differential thermal analysis. Accordingly, samples have been annealed at different temperatures. Infrared studies revealed formation of Cu-ZnO nanoparticles and removal of organic matter at higher temperature.
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