Journal
JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
Volume 93, Issue 3, Pages 759-762Publisher
SPRINGER
DOI: 10.1007/s10973-008-9141-9
Keywords
cathode materials; DTA; Li-ion batteries; lithium-iron phosphate glasses; phospho-olivines
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Amorphous analogs of lithium-iron phosphates (LFP) were prepared by standard press-quenching method and their thermal stabilities as well as structural properties were studied for the first time. Glass transition temperature T-g determined by DTA method was observed at the temperature range 492-523 degrees C, depending on the glass composition. The maxima of crystallization peaks were observed in the 555-579 degrees C range. In products obtained after heating LIP to 700 degrees C the XRD patterns have revealed the presence of: LiFePO4 (triphylite), FePO4 (heterosite), alpha-FePO4 (quartz like structure) and Li3Fe2(PO4)(3) (Nasicon like structure) phases.
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