Journal
JOURNAL OF THE ELECTROCHEMICAL SOCIETY
Volume 159, Issue 4, Pages E82-E86Publisher
ELECTROCHEMICAL SOC INC
DOI: 10.1149/2.033204jes
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Funding
- Bu-Ali Sina University Research Council
- Center of Excellence in Development of Chemical Methods (CEDCM)
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Electrochemical oxidation of 4-(piperazin-1-yl)phenol has been studied in the presence of aryl sulfinic acids as nucleophiles in ethanol/water mixture (10/90) using cyclic voltammetry and controlled-potential coulometry methods. The results indicate that the electrochemically generated p-quinone-imine participates in Michael type addition reaction with aryl sulfinic acids and via an EC mechanism converts to the new 2-(phenylsulfonyl)-4-(piperazin-1-yl)phenol derivatives. The present work has led to the development of a facile and environmentally friendly electrochemical method for the synthesis of some new 2-(phenylsulfonyl)-4-(piperazin-1-yl)phenol derivatives under green conditions. (C) 2012 The Electrochemical Society. [DOI: 10.1149/2.033204jes] All rights reserved.
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