Journal
JOURNAL OF THE CHINESE CHEMICAL SOCIETY
Volume 56, Issue 1, Pages 150-157Publisher
CHINESE CHEMICAL SOC
DOI: 10.1002/jccs.200900021
Keywords
Surfactant coated alumina; Atomic absorption spectrometry; Solid phase extraction
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Funding
- Graduate School and Research Council of the University of Yasouj
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A sensitive and simple method for the simultaneous preconcentration of trace transition and heavy metal ions is reported. The method is based on the adsorption of Cu, Fe, Pb and Zn on N,N'-Diacetyl-4-bromo-2,6-di(aminomethyl)anisole (DABDAMA) loaded on sodium dodecyl sulfate (SDS) coated alumina. The metal content on the complexes are eluted using 6 mL of 2 mol l(-1) nitric acid. The influences of the analytical parameters including pH and sample volume were investigated. The effects of matrix ions on the retentions of the analytes were also examined. The recoveries of analytes were generally higher than 95% with a low RSD. The method has been successfully applied for these metals content evaluation in samples including soil, blood and vegetable samples.
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