Journal
JOURNAL OF THE BRAZILIAN CHEMICAL SOCIETY
Volume 22, Issue 7, Pages 1259-1262Publisher
SOC BRASILEIRA QUIMICA
DOI: 10.1590/S0103-50532011000700010
Keywords
monoterpenes; allylic chlorination; molybdenum; sodium hypochlorite
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MoCl5 is applied as efficient agent in allylic chlorination of terpenic olefins in the presence of NaOCl as chlorine donor. Various terpenes are converted to the corresponding allylic chlorides in moderate to good yield under mild and optimized reaction conditions. Different molybdenum precursors are also studied. Among them, MoO3 gives good yield, but after a longer reaction time.
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