Journal
JOURNAL OF THE AMERICAN SOCIETY FOR MASS SPECTROMETRY
Volume 24, Issue 5, Pages 684-689Publisher
SPRINGER
DOI: 10.1007/s13361-012-0513-9
Keywords
MALDI; TOF/TOF; Charge-remote fragmentation; High-energy CID; Triacylglycerols; MS/MS; Lipids; Collision-induced dissociation
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A new MALDI-TOF/TOF system with monoisotopic precursor selection was applied to the analysis of triacylglycerols in an olive oil sample. Monoisotopic precursor selection made it possible to obtain product-ion mass spectra without interference from species that differed by a single double bond. Complete structure determination of all triacylglycerols, including structural isomers, was made possible by interpreting the charge-remote fragmentation resulting from high-energy collision-induced dissociation (CID) of the sodiated triacylglycerols.
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