Journal
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
Volume 135, Issue 46, Pages 17302-17305Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ja409941r
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Funding
- National Basic Research Program of China [2012CB821600, 2012CB215500]
- National Natural Science Foundation of China [21372246, 20825209]
- MSD China R&D Postdoc Fellowship
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A novel Cu-catalyzed gem-difluoroolefination of diazo compounds is described. This transformation starts from readily available TMSCF3 and diazo compounds, via trifluoromethylation followed by C-F bond cleavage, to afford the desired 1,1-difluoroalkene products.
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