Journal
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
Volume 134, Issue 44, Pages 18237-18240Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ja3092278
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Funding
- Welch Foundation [E-1571]
- National Institute of General Medical Science [R01GM077635]
- Camille and Henry Dreyfus Foundation
- Norman Hackerman Advanced Research Program
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An auxiliary-assisted, copper catalyzed or promoted sulfenylation of benzoic acid derivative beta-C-H bonds and benzylamine derivative gamma-C-H bonds has been developed. The method employs disulfide reagents, copper(II) acetate, and DMSO solvent at 90-130 degrees C. Application of this methodology to the direct trifluoromethylsulfenylation of C-H bonds was demonstrated.
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