Journal
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
Volume 133, Issue 39, Pages 15308-15311Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ja2064395
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Funding
- National Institutes of Health [R01 GM08525]
- John M. Witt Jr. Fellowship
- Alexander von Humboldt Foundation
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Catalytic asymmetric sulfenylation of double bonds has been achieved using a BINAM-based phosphoramide catalyst and an electrophilic sulfur source. Simple alkenes as well as styrenes afforded sulfenylated tetrahydrofurans and tetrahydropyrans by closure with pendant hydroxyl or carboxyl groups. Intermolecular thiofunctionalizations were also achieved with simple alcohols or carboxylic acids as the nucleophiles.
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