4.8 Article

Preparation and Characterization of a Tetrabutylammonium Graphite Intercalation Compound

Journal

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
Volume 133, Issue 32, Pages 12436-12438

Publisher

AMER CHEMICAL SOC
DOI: 10.1021/ja2053539

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The intercalation of tetrabutylammonium (TBA) cations into graphite by cation exchange from a sodium-ethylenediamine graphite intercalation compound yields a single-phase first-stage product, C(44)TBA, with a gallery expansion of 0.47 nm. The gallery dimension requires an anisotropic flattened cation conformation.

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