Journal
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
Volume 133, Issue 6, Pages 1775-1777Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ja110864t
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Funding
- NNSFC [21072027]
- Young Scientific Research Foundation of Jilin Province [20090149]
- Fundamental Research Funds for the Central Universities [09 QNJJ017]
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A new strategy for the construction of the compounds with two different heterocycles, linked by a C(2)-tether via a domino process involving [5 + 1] annulation, ring-opening, and subsequent double isocyanide cyclization, from the reaction of ethyl isocyanoacetate with divinyl ketones (DVKs) has been developed. The chemoselective fragmentation of the cyclohexanone intermediate is the key for the formation of not only the C(2)-tether but also the two different heterocycles.
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