Journal
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
Volume 133, Issue 33, Pages 12984-12986Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ja206002m
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Funding
- Ministry of Education, Culture, Sports, Science and Technology (MEXT), Japan
- JSPS
- Grants-in-Aid for Scientific Research [22105001, 10J00248, 22245016] Funding Source: KAKEN
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The first catalytic alkynylation of unactivated C(sp(3))-H bonds has been accomplished. The method allows for the straightforward introduction of an ethynyl group into aliphatic acid derivatives under palladium catalysis. This new reaction can be applied to the rapid elaboration of complex aliphatic acids, for example, via azide/alkyne cycloaddition.
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