Journal
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
Volume 133, Issue 23, Pages 8818-8821Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ja201794v
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Funding
- NSFC [20921120404, 20732002, 20972059]
- 973 program [2010CB833200]
- MOE
- fundamental research funds for the central universities [lzujbky-2010-k09, lzujbky-2009-76, lzujbky-2009-158]
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A novel asymmetric halogenation/semipinacol rearrangement reaction catalyzed by cinchona alkaloid derivatives was developed. Two types of beta-haloketones (X = Br, Cl) were obtained with up to 95% yield and 99% enantiomeric excess. The desired (+) and (-) enantiomers of the beta-haloketones were readily obtained.
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