Journal
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
Volume 133, Issue 44, Pages 17638-17640Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ja209300c
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Funding
- MEXT (KAKENHI Specially Promoted Research) [22000008, 23750100]
- Global COE Program for Chemistry Innovation
- Japan Society for the Promotion of Science [P10033]
- Grants-in-Aid for Scientific Research [22000008, 10F00033, 23750100] Funding Source: KAKEN
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A variety of polysubstituted 1H-indenes can be prepared through the copper-catalyzed arylative cyclization of simple arylalkynes with commercially available aromatic sulfonyl chlorides that function as an aryl group donor. The reaction tolerates a broad range of. functional groups, including bromide and iodide, nitrile, ketone, and nitro groups. The reaction allowed the synthesis. of poly-cyclic aromatic hydrocarbons, such; as a bis(indene), indacene, and fused polyarene derivatives, some of them showing strong fluorescence in solution and the solid state.
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