Journal
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
Volume 132, Issue 8, Pages 2839-2844Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ja910586v
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Funding
- National Science Foundation [CHE-0809142, RR02004, RR05018, RR07155]
- Washington University High Resolution NMR facility
- Washington University Mass Spectrometry Resource Center [NIHRR00954]
- Direct For Mathematical & Physical Scien
- Division Of Chemistry [0809142] Funding Source: National Science Foundation
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Anodic olefin coupling reactions using a tosylamine trapping group have been studied. The cyclizations are favored by the use of a less-polar radical cation and more basic reaction conditions. The most significant factor for obtaining good yields of cyclic product is the use of the more basic reaction conditions. However, a number of factors including the nature of both the solvent and the electrolyte used can influence the yield of the cyclizations. The cyclizations allow for the rapid synthesis of both substituted proline and pipecolic acid type derivatives.
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