Journal
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
Volume 131, Issue 7, Pages 2615-2620Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ja807769r
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Funding
- National Science Foundation [CHE-0533150, CHE-9808061, DBI-9729592]
- Chesonis Family Foundation
- Department of Defense
- Direct For Mathematical & Physical Scien
- Division Of Chemistry [0802907] Funding Source: National Science Foundation
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Electrolysis of CO2+ in phosphate, m ethyl phosphonate, and borate electrolytes effects the electrodeposition of an amorphous highly active water oxidation catalyst as a thin film on an inert anode. Electrodeposition of a catalytically competent species immediately follows oxidation of CO2+ to CO3+ in solution. M ethyl phosphonate and borate electrolytes support catalyst activity comparable to that observed for phosphate. Catalytic activity for O-2 generation in aqueous solutions containing 0.5 M NaCl is retained for catalysts grown from phosphate electrolyte.
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