Journal
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
Volume 131, Issue 1, Pages 12-+Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ja805521y
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Funding
- National Institutes of Health [EB002804, EB002026]
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Dynamic nuclear polarization is combined with temperature-jump methods to develop a new 2D C-13-C-13 NMR experiment that yields a factor of 100-170 increase in sensitivity. The polaization step is performed at similar to 100 K, and the sample is subsequently melted with a 10.6 mu m laser pulse to yield a sample with highly polarized C-13 spins. C-13 detected 2D C-13-C-13 spectroscopy is performed in the usual manner.
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