4.8 Article

A Structural Resolution Cryo-TEM Study of the Early Stages of MFI Growth

Journal

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
Volume 130, Issue 51, Pages 17284-+

Publisher

AMER CHEMICAL SOC
DOI: 10.1021/ja8063167

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Funding

  1. NSF [NIRT-CMMI-0707610, CBET-0522518, MRSEC: DMR-0212302]
  2. China Scholarship Council

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Room-temperature aging of zeolite precursor silica sol was followed by SAXS and cryo-TEM. Cryo-TEM imaging of zeolite materials with structural resolution is demonstrated. The results suggest the formation of predominantly amorphous aggregates before MFI crystallization.

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