Journal
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
Volume 130, Issue 17, Pages 5662-+Publisher
AMER CHEMICAL SOC
DOI: 10.1021/ja801655d
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Pyridine ring opening occurs in the reaction of [Re(CO)(3)(Melm)(bipy)] OTf with KN(SiMe3)2 followed by double methylation with methyl trifluoromethanesulfonate. Analogues of the neutral product of the initial deprotonation and of the product of the first methylation were isolated by using mesitylimidazole (Meslm) in place of methylimidazole (Melm) and/or 1,10-phenanthroline (phen) instead of 2,2'-bipyridine (bipy).
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