Journal
JOURNAL OF THE AMERICAN CERAMIC SOCIETY
Volume 95, Issue 4, Pages 1320-1325Publisher
WILEY
DOI: 10.1111/j.1551-2916.2012.05117.x
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Funding
- Natural Science Foundation of China [61108057]
- Zhejiang Provincial Natural Science Foundation of China [R1101263, Y4110322]
- Program for Innovative Research Team in Ningbo City [2009B21007]
- Natural Science Foundation of Ningbo City [2011A610091]
- Program for New Century Excellent Talents in University [NCET-10-0976]
- outstanding Dissertation Engagement Foundation of Graduate School of Ningbo University [PY20100010]
- Ningbo University
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54GeS(2)-36Sb(2)S(3)-10In(2)S(3) glass-ceramics were prepared by heat-treating the base glass above T-g for different durations. The results of Raman spectra and XRD patterns show that the first precipitated crystals during the heat treatment are In2S3 and the crystallization of the Sb2S3 and GeS2 subsequently occurs. Bulk samples heat-treated at 295 degrees C for different heating rates and durations are used to study the crystallization mechanism and evolution of the three crystallization peaks (CPs). It is found that three CPs partly overlap with each other and then separate with increasing heat-treating durations.
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