Journal
JOURNAL OF THE AMERICAN CERAMIC SOCIETY
Volume 95, Issue 11, Pages 3377-3379Publisher
WILEY-BLACKWELL
DOI: 10.1111/j.1551-2916.2012.05458.x
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Funding
- Fundamental Research Funds of the Central University
- Science and Technology Planning Project from Education Department of Heilongjiang Province [11553044]
- China Postdoctoral Science Foundation [AUGA41309003]
- Special Innovation Talents of Harbin Science and Technology [2010RFXXG007]
- foundation of Harbin Engineering University [HEUFT07053]
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Flower-like hydroxyapatite (HA) was prepared by a solvothermal method using calcined eggshells as calcium source and hydrogen peroxide/N,N-dimethylformamide (DMF) as solvent. The products are characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), and Scanning electron microscopy (SEM). All the above-mentioned instrumental analysis such as XRD and FT-IR showed the purity of HA. The SEM indicates that the as-obtained flower-like HA are composed of microsheets. These nanosheets interleaved each other to form the uniform flower-like morphology. The influence of precipitation temperature and ratio of hydrogen peroxide to DMF were systematically investigated by SEM analysis.
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