4.2 Article

I18-the microfocus spectroscopy beamline at the Diamond Light Source

Journal

JOURNAL OF SYNCHROTRON RADIATION
Volume 16, Issue -, Pages 818-824

Publisher

WILEY-BLACKWELL PUBLISHING, INC
DOI: 10.1107/S0909049509032282

Keywords

microfocus; EXAFS; Diamond; XANES; X-ray fluorescence

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The design and performance of the microfocus spectroscopy beamline at the Diamond Light Source are described. The beamline is based on a 27 mm-period undulator to give an operable energy range between 2 and 20.7 keV, enabling it to cover the K-edges of the elements from P to Mo and the L(3)-edges from Sr to Pu. Micro-X-ray fluorescence, micro-EXAFS and micro-X-ray diffraction have all been achieved on the beamline with a spot size of similar to 3 mu m. The principal optical elements of the beamline consist of a toroid mirror, a liquid-nitrogen-cooled double-crystal monochromator and a pair of bimorph Kirkpatrick-Baez mirrors. The performance of the optics is compared with theoretical values and a few of the early experimental results are summarized.

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