Journal
JOURNAL OF SULFUR CHEMISTRY
Volume 32, Issue 5, Pages 405-412Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/17415993.2011.608799
Keywords
tetrazinanethiones; thiocarbohydrazide; monothiocarbohydrazone; electron-deficient alkynes; thiazolidinone
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Funding
- Yarmouk University
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Aliphatic aldehydes and cyclohexanone reacted with thiocarbohydrazide to give exclusively 6-substituted-1,2,4,5-tetrazinane-3-thiones, which readily underwent cyclization with diethyl acetylene dicarboxylate to afford condensed thiazolidinones. On the other hand, cyclopentanone and cycloheptanone reacted under a similar sequence of reaction conditions to give 3-amino thiazolidin-4-ones. [GRAPHICS] .
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