Journal
JOURNAL OF SOLID STATE CHEMISTRY
Volume 184, Issue 9, Pages 2345-2352Publisher
ACADEMIC PRESS INC ELSEVIER SCIENCE
DOI: 10.1016/j.jssc.2011.06.020
Keywords
Nanoparticles; Metathesis reaction; X-ray absorption spectroscopy
Funding
- Wolfson Foundation-Royal Society
- EPSRC [EP/D07357X, EP/D504782]
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We present results of an XAS and EXAFS study of the synthesis of Ge nanoparticles formed by a metathesis reaction between Mg2Ge and GeCl4 in diglyme (diethylene glycol dimethyl ether). The progress of the formation reaction and the products formed at various stages in the processing was characterised by TEM and optical spectroscopy as well as in situ XAS/EXAFS studies using specially designed reaction cells. (C) 2011 Elsevier Inc. All rights reserved.
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