Journal
JOURNAL OF SOLID STATE CHEMISTRY
Volume 182, Issue 6, Pages 1550-1555Publisher
ACADEMIC PRESS INC ELSEVIER SCIENCE
DOI: 10.1016/j.jssc.2009.03.026
Keywords
Metal phosphide; Synthesis; Hydrogen plasma; Reduction; Non-thermal
Funding
- NSFC [20333030, 20503003, 20773020]
- NCET
- 111 Project
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A series of transition metal phosphides, including MoP, WP, CoP, Co2P, and Ni2P, were synthesized from their oxidic precursors by means of hydrogen plasma reduction under mild conditions. The effects of reduction conditions, such as metal to phosphorus molar ratio, power input, and reduction time, on the synthesis of metal phosphides were investigated. The products were identified by means of XRD characterization. It is indicated that metal phosphides were readily synthesized stoichiometrically from their oxides in hydrogen plasma under mild conditions. (C) 2009 Elsevier Inc. All rights reserved.
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