Journal
JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY
Volume 60, Issue 2, Pages 198-205Publisher
SPRINGER
DOI: 10.1007/s10971-011-2579-4
Keywords
Iron oxides; Nanoparticles; Microwave heating; XRD; TEM; FTIR; XPS
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A simple, rapid, one-step synthesis way of pure iron oxide nanoparticles: magnetite (Fe3O4), maghemite (c-Fe2O3) and hematite (alpha-Fe2O3) was investigated. Nanoparticles were prepared by microwave synthesis, from ethanol/water solutions of chloride salts of iron (FeCl2 and FeCl3) in the presence of sodium hydroxide NaOH. X-ray powder diffraction (XRD), Transmission Electron Microscopy (TEM), Fourier transform infrared (FTIR) spectroscopy and X-ray photoelectron spectroscopy (XPS) were used to characterize these nanoparticles.
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