Journal
JOURNAL OF SEPARATION SCIENCE
Volume 38, Issue 1, Pages 108-114Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/jssc.201400814
Keywords
Curcumin; Magnetic materials; Molecularly imprinted polymers; Multi-walled carbon nanotubes; Solid-phase extraction
Categories
Funding
- National Natural Science Foundation of China [21005030, 21267010]
- State Key Laboratory of Environmental Chemistry and Ecotoxicology [KF2011-25]
- Construct Program of the Key Discipline in Hunan Province [JSU0713Z31]
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A novel molecularly imprinted polymer based on magnetic phenyl-modified multi-walled carbon nanotubes was synthesized using curcumin as the template molecule, methacrylic acid as the functional monomer and ethylene glycol dimethacrylate as the cross-linker. The phenyl groups contained in the magnetic imprinted polymers acted as the assisting functional monomer. The magnetic imprinted polymers were characterized by scanning electron microscopy, Fourier-transform infrared spectroscopy and vibrating sample magnetometry. Adsorption studies demonstrated that the magnetic imprinted polymers possessed excellent selectivity toward curcumin with a maximum capacity of 16.80 mg/g. Combining magnetic extraction and high-performance liquid chromatography technology, the magnetic imprinted polymer based on magnetic phenyl-modified multi-walled carbon nanotubes was applied for the rapid separation and enrichment of curcumin from ginger powder and kiwi fruit root successfully.
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