Journal
JOURNAL OF SEPARATION SCIENCE
Volume 33, Issue 16, Pages 2394-2401Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/jssc.201000137
Keywords
Amino acids; Clinical samples; Contactless conductivity detection; Short pathway separation
Categories
Funding
- Grant Agency of the Czech Republic [P206/10/1231]
- Ministry of Education, Youth and Sports, Czech Republic [MSM0021620814]
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CE with contactless conductivity detection has been used to separate 28 biogenic amino acids in a short capillary with an effective length of 18 cm. All the tested amino acids can be mutually separated in 0.5-10 mol/L acetic acid electrolytes. The time of analysis does not exceed 6 min and the LODs vary from 0.1 to 1.7 mu mol/L. The CVs lie within the intervals 0.01-0.4% and 0.9-4% for the migration times and the analyte peak areas, respectively. The procedure has been successfully applied to the determinations of the whole amino acid spectra in blood plasma, urine, saliva and cerebrospinal fluid samples.
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