Journal
JOURNAL OF SEPARATION SCIENCE
Volume 32, Issue 19, Pages 3327-3333Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/jssc.200900307
Keywords
Molecularly imprinted microparticles; Permselective binding; Surfactant-free dispersion polymerization; alpha-Tocopherol
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alpha-Tocopherol (alpha-Toc) targeted membrane adsorbents were priepared by mixing alpha-Toc imprinted particles in polysulfone (PSf) scaffold. The alpha-Toc imprinted particles were prepared with high-shear dispersion copolymerization of alpha-Toc methacrylate (alpha-TMA) and divinylbenzene (DVB) in toluene and water in the agitation range of 300-13 500 rpm. The alpha-Toc groups in resultant imprinted particles were hydrolyzed with 2 M HCI and then the polymers were embedded in PSf membranes by phase inversion technique. The membrane exhibited good selective binding of alpha-Toc with high separation factors to its analogs.
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