4.6 Article

On-wafer time-dependent high reproducibility nano-force tensile testing

Journal

JOURNAL OF PHYSICS D-APPLIED PHYSICS
Volume 47, Issue 49, Pages -

Publisher

IOP Publishing Ltd
DOI: 10.1088/0022-3727/47/49/495306

Keywords

nano-force micro-tensile testing; anelasticity; creep; thin films; global digital image correlation; in situ micromechanical characterization

Funding

  1. Industrial Partnership Program on Size Dependent Material Properties of the Materials innovation institute M2i [M62.2.08SDMP12]
  2. Foundation of Fundamental Research on Matter (FOM), Netherlands Organisation for Scientific Research (NWO)

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Time-dependent mechanical investigations of on-wafer specimens are of interest for improving the reliability of thin metal film microdevices. This paper presents a novel methodology, addressing key challenges in creep and anelasticity investigations through on-wafer tensile tests, achieving highly reproducible force and specimen deformation measurements and loading states. The methodology consists of a novel approach for precise loading using a pinin- hole gripper and a high-precision specimen alignment system based on three-dimensional image tracking and optical profilometry resulting in angular alignment of < 0.1 mrad and near-perfect co-linearity. A compact test system enables in situ tensile tests of on-wafer specimens under light and electron microscopy. Precision force measurement over a range of 0.07 mu N to 250 mN is realized based on a simple drift-compensated elastically-hinged load cell with high-precision deflection measurement. The specimen deformation measurement, compensated for drift through image tracking, yields displacement reproducibility of < 6 nm. Proof of principle tensile experiments are performed on 5 mu m-thick aluminum-alloy thin film specimens, demonstrating reproducible Young's modulus measurement of 72.6 +/- 3.7 GPa. Room temperature creep experiments show excellent stability of the force measurement and underline the methodology's high reproducibility and suitability for time-dependent nanoforce tensile testing of on-wafer specimens.

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